A reaction conducted in my inorganic chemistry II class. The solution is of a Ru(bipy)2 complex and magnesium is added for the reaction. The reaction...
trans-9-(2-phenylethenyl)anthracene (10mg) with alumina(1g), DCM (5mL) 3% H2O2 (1mL), Oxalyl Chrloride (.015mL) and a further DCM (3mL). My Latest CHEM330 lab :D
Two solutions, A and B, are made. Solution A contains Luminol in an alkaline environment, whilst solution B contains Potassium Ferricyanide in a 0,03% Hydrogen...
3-Nitrophthalhydrazide, prepared in a previous video, is reduced with a readily available reducing agent (thiourea dioxide, TUD) to luminol, which is obtained in 66% yield...
A necessary precursor to luminol, 3-nitrophthalic acid, is prepared by mixed acid nitration of phthalic anhydride. The product is obtained in 35% yield with purity...
